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Assay Results Confirm High Grade Mineralisation

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Altona Rare Earths PLC has announced final assay results from its 2025 drilling campaign at Monte Muambe, confirming high-grade, near-surface fluorspar and gallium mineralization. The company reported a record fluorspar intercept of 30 metres at 42.5% CaF₂, with a weighted average grade of 30% CaF₂ across all significant intercepts, aligning with commercial mining benchmarks. Gallium mineralization was encountered in consistent intercepts averaging 18 metres, with a weighted average grade of 63 g/t Ga₂O₃, exceeding expectations. Metallurgical testing for gallium recovery from fluorspar tailings is now underway, and the company is focused on delivering a Mineral Resource Estimate.

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Altona (LSE: REE), a resource exploration and development company focused on critical raw materials in Africa, is pleased to announce the receipt of all outstanding assay results from its 2025 drilling campaign at Monte Muambe.

Highlights

  • All assays received: Final results from the 2025 drilling programme are now in hand, clearing the path for the delivery of the Mineral Resource Estimate ("MRE").
  • Record fluorspar intercept: Hole MM156 returned 30 metres at 42.5% CaF₂ from surface, representing the highest grade × intercept length recorded to date at the Monte Muambe project.
  • Consistent, commercial-grade fluorspar: The weighted average grade of all significant fluorspar intercepts is 30% CaF₂, aligning with industry benchmarks for commercially viable open-pit mining operations (typically 20-40% CaF₂).
  • Gallium results exceed expectations: Gallium mineralisation was encountered over wide, consistent intercepts up to 50 metres (averaging 18 metres), with a weighted average grade of 63 g/t Ga₂O₃. These results surpassed internal pre-drilling expectations.
  • Gallium metallurgical testing underway: A gallium metallurgical testing programme was initiated last week to assess recovery potential from fluorspar tailings, an essential step toward evaluating commercial viability.

Received results correspond to samples from diamond drilling and reverse circulation drilling holes at the Fluorite Zone, Southern Extension, Kudu and Python.

It is noteworthy that the 2025 drilling campaign covered only about 40% surface area of soil gallium and fluorspar anomalies. The remaining 60% has not been drilled yet, leaving significant scope for new mineralized zones identification and definition through additional drilling.

Individual sample grades reach up to 93.11% CaF2 and up to 149 g/t Ga2O3.

Significant intercepts for fluorspar and gallium are detailed in the tables below.

Fluorspar Results Meet Expectations

The weighted average of the fluorspar intercepts reported in this RNS which cover 2,842 reverse circulation drilling samples is 30% CaF2, with numerous surface or near-surface intercepts, confirming a favourable geometry for open-pit mining. This is consistent with the Company's pre-drill expectations for this project as well as with grades at which fluorspar is commercially mined, typically ranging from 20% to 40% CaF2.

Results include a record fluorspar intercept (in terms of grade x intercept length) for hole MM156, with 30m at 42.5% CaF2.

Gallium Results Exceed Expectations

Gallium results show consistent mineralisation with grades above 55 g/t Ga2O3 across wide intercepts (up to 50m, average 18m). The weighted average grade of the gallum intercepts is 63 g/t Ga2O3.

Gallium results strongly exceed the Company's pre-drilling expectations. Gallium grades extend into the host rock of fluorspar mineralisation, meaning that gallium may be recovered not only from fluorspar ore but also from fluorspar waste. These results underpin the importance of specific gallium metallurgical testing workstreams initiated by the Company as announced on 19 March 2026.

Next steps

All assay results have now been incorporated in the project database and work towards the preparation of the MRE is on-going. The Company will provide further updates as this work progresses, alongside results from the gallium metallurgical testing programme.

Cedric Simonet, CEO, commented: "These final assay results give us a complete picture of the 2025 resource drilling campaign and have confirmed the high-grade nature of fluorspar mineralization at Monte Muambe aligned with our expectations.

"Gallium results, however, show an exceptional consistency and exceeded our expectations. While gallium associated to carbonatites and fluorspar is a new type of deposit, and much work remains to be done to establish its ultimate commercial viability, these results clearly strengthen the case for investing further in gallium studies. The initiation of gallium metallurgical testing announced last week is a essential part of these studies.

"With all assays now in hand, we are focused entirely on delivering the MRE. That will be the next major milestone in building a comprehensive understanding of Monte Muambe's value."

Significant fluorspar intercepts (over 18% CaF2):

Hole NumberFrom (m)Length (m)CaF 2 %
MM12712856.6%
MM12725834.7%
MM12829719.6%
MM1301632.1%
MM130281546.7%
MM1313321.1%
MM131271427.3%
MM134Surface2519.5%
Including1536.6%
Including12342.2%
MM13591634.2%
MM136Surface1342.0%
MM13624519.1%
MM13638721.5%
MM138Surface1023.9%
IncludingSurface537%
MM13831421.1%
MM138482*62.6%
MM139Surface1429.4%
MM139231018.1%
MM1431425.4%
MM14317526.8%
MM144Surface318.7%
MM14632430.6%
Including151240.7%
MM148Surface2632.0%
MM1501430.4%
MM151191132.8%
MM15231830.3%
MM15318424.5%
MM156Surface3042.5%
Including61254.7%
MM16023418.9%
MM16181118.1%
MM1626326.5%
MM16225421.4%
MM1631553.9%
MM16858823.3%
MM169732*28.8%
MM17021622.2%
MM17034820.2%
MM17059728.5%
MM173381226.8%
MM17527427.7%
MM1798623.9%
MM182151127.6%
MM18229521.5%
MM182594*19.3%
MM183202432.2%
Including24741.8%
Including36442.7%
MM18349931.6%
MM18421728.4%

* Hole ended in mineralisation, open at depth.

Significant gallium intercepts (over 54g/t Ga2O3):

Hole NumberFrom (m)Length (m)Ga 2 O 3 g/t
MM125281163
MM12710368
MM128Surface562
MM128151358
MM12928664
MM131Surface2163
MM131271962
Including38878
MM13212367
MM137Surface1960
MM13853371
Including271184
MM13923864
Including32878
MM140Surface2859
MM14822852
MM150282265
MM15231564
MM15491855
MM15512461
MM15712467
Including195111
MM15821879
MM159231573
MM16012259
MM16111552
MM16223758
MM166Surface2167
MM16721069
MM168212262
MM16854856
MM16873962
MM16920558
MM169361958
Including514100
MM16965963
MM170Surface878
MM17015465
MM170351167
MM170522667
MM171132058
MM171541456
MM172292557
MM17381863
MM173431484
MM17364665
MM174Surface2180
MM174641662
MM175Surface858
MM175141255
MM175332354
MM17612058
MM176262465
MM177174361
MM178282767
MM179Surface5059
MM18025397
MM18034679
MM18146555
MM182431856
MM18362070

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Altona Rare Earths Plc

Cédric Simonet, CEO +44 (0) 7778 866 108 (cs@altonare.com)

Louise Adrian, CFO +44 (0) 7721 492 922 (la@altonare.com)

Strand Hanson (Financial Adviser) +44 (0) 20 7409 3494

Christopher Raggett

Imogen Ellis

Zeus Capital (Corporate Broker) +44 (0) 20 3829 5000

Simon Johnson

James Hornigold

About Altona Rare Earths Plc

The multi-commodity Monte Muambe Project in northwest Mozambique is a highly prospective tenement hosting rare earths, fluorspar, and gallium mineralisation. Since acquiring the project in June 2021, Altona has drilled over 7,800 metres, delivering a maiden JORC Mineral Resource Estimate of 13.6Mt at 2.42% TREO, secured a 25-year mining licence (granted December 2024), and published a Competent Person Report and scoping study for the rare earths component of the project (October 2023). The Company has received a US$ 1.875 million grant from USTDA to advance the rare earths project through the prefeasibility stage.

In parallel, Altona is progressing plans to fast-track the development of high-grade fluorspar veins identified along the western and southern margins of Monte Muambe, with a targeted production of 50,000 tonnes per annum of acid-grade fluorspar over a minimum 12-year mine life. Acid-grade fluorspar is a key input in a wide range of applications, including hydrofluoric acid, lithium battery electrolyte production, and nuclear fuel refining, placing Altona in a strong position to supply this critical material.

Cleaned text: letterheads, contacts and legal notices removed. View the original announcement ↗ · Company filings. Not investment advice.

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